HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19433627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 70302783 | HCID 70302783 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19433627 | HCID 19433627 | 41% |
Reaction Steps
5,5'-[2,5-furandiylbis(carbonylimino)]bis-1H-indole-2-carboxylic acid diethyl ester (60 mg, 0.11 mM) is suspended in methanol (0.4 mL) and treated with N NaOH (0.25 mL). After 5 days the reaction is evaporated in vacuo and the residue dissovlved in water and the solution acidified to pH 2 with N HCl. This solution is freeze dried leaving 5,5'-[2,5-furandiylbis(carbonylimino)]bis-1H-indole-2-carboxylic acid (22 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05541339 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-37317e8f7b274a8f82523f39354974e4 |
| Source note | uspto-grants-1996_07 |