HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-t-Butylbenzenesulfonyl chloride → Benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-t-Butylbenzenesulfonyl chloride | HCID 139882 | — |
| Reactant | Pyridine toluene | HCID 22007288 | — |
| Product | Benzenesulfonamide | HCID 7370 | — |
Reaction Steps
Reaction with p-tert-butylbenzenesulphonyl chloride in pyridine/toluene at room temperature yielded pure 4-tert-butyl-N-[3-(2-tetrahydropyranyloxyethoxy)-2-methoxy-phenoxy)-phenyl]-benzenesulphonamide. MS: Mt /e=555.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962682 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-18a535080f7247fd8430b79d0b11a6e1 |
| Source note | uspto-grants-1999_10 |