HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 11084708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 54119352 | HCID 54119352 | — |
| Product | HCID 11084708 | HCID 11084708 | — |
Reaction Steps
According to the same manner as that described in Reference Example 10, ethyl 4-isopropoxycinnamate was reduced with diisobutyl aluminum hydride to give (E)-3-(4-isopropoxyphenyl)-2-propenol as an oil. This oil was purified by column chromatography on silica gel (eluent: ethyl acetate-hexane (1:4, v/v)) (yield: 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965589 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-b0375b4162f34d26a68474a95d04a71a |
| Source note | uspto-grants-1999_10 |