HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11118803, compound → HCID 10998484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11118803 | HCID 11118803 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Product | HCID 10998484 | HCID 10998484 | 76% |
Reaction Steps
According to the same manner as that described in Reference Example 10, ethyl (E,E)-5-(4-isopropoxyphenyl)-2,4-pentadienoate was reduced with diisobutyl aluminum hydride to give crystals of (E,E)-5-(4-isopropoxyphenyl)-2,4-pentadienol (yield: 76%). The crystals were recrystallized from isopropyl ether. Colorless needles, mp: 91-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965589 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-d32ad856f75d475fbf9b33ce6222e8bf |
| Source note | uspto-grants-1999_10 |