HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → HCID 178447298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | HCID 53687967 | HCID 53687967 | — |
| Product | HCID 178447298 | HCID 178447298 | — |
Reaction Steps
N-valeryl-N-[(2'-cyanobiphenyl-4-yl)methyl]-(L)-alanine methyl ester starting from 1.65 g of N-[(2'-cyanobiphenyl)-methyl]-(L)-alanine methyl ester, 2.7 ml of triethylamine and 2.35 ml of n-valeryl chloride and subsequent flash chromatography (N2). (TLC: system N2) Rf : 0.62.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965592 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-9b3763e6a6f64454b5550f9525ce80d6 |
| Source note | uspto-grants-1999_10 |