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HRID1739154

反应详情

EQUATION

反应方程式

HRID 1739154 的结构方程式

REACTANTS

反应物

3
结构：CSCC[C@H](N)C(=O)O
HCID6137

L-Methionine

C5H11NO2S

结构：COC(=O)[C@@H](N)CC(C)C.Cl
HCID2723695

Methyl L-leucinate hydrochloride

C7H16ClNO2

结构：O=C(O)c1ccc([N+](=O)[O-])cc1-c1ccccc1
HCID10657841

4-NITRO-2-PHENYLBENZOIC ACID

C13H9NO4

PRODUCTS

生成物

1
结构：COC(=O)[C@H](CC(C)C)NC(=O)c1ccc([N+](=O)[O-])cc1-c1ccccc1
HCID10642898

未命名化合物

PROCEDURE

实验过程

This compound was prepared through the coupling of 4-nitro-2-phenylbenzoic acid with (L)-leucine methyl ester hydrochloride as for the preparation of the methionine derivative (see Example 26, section A). 1H NMR (CDCl3) δ 8.24-8.26 (m, 2H), 7.86 (d, 8.7 Hz, 1H), 7.41-7.46 (m, 5H), 5.71 (d, 7.4 Hz, 1H), 4.57 (ddd, 1H), 3.67 (s, 3H), 1.37-1.46 (m, 1H), 1.08-1.25 (m, 2H), 0.78 (dd, 6H).