Acridine → HCID 178420595, compound

Participants

Reaction Steps

To a solution of 5.00 g (17.10 mmol) zirconocene dichloride in 100 ml THF were added 3.06 g (17.10 mmol) acridine and 0.41 g magnesium and the mixture was stirred at room temperature until the metal was fully reacted. The solvent was then removed to dryness in vacuo and the residue was extracted with 80 ml toluene. 4.29 g bis(cyclopentadienyl)zirconium acridine were isolated from the toluene extract as a red solid.

Provenance & Evidence