Thionyl Chloride → HCID 21841066, compound

Participants

Reaction Steps

1.67 g of 4-[3-(4-tolyloxy)propyloxy]benzyl alcohol were dissolved in 30 ml of chloroform, and the resultant solution was then stirred for 1 hour at room temperature after conducting the dropping of 0.88 g of thionyl chloride into the solution. The solution reacted was then poured into ice-water and extracted with chloroform, and the organic layer resulted was dried with anhydrous magnesium sulfate, and the solvent used was removed by distillation under reduced pressure thereby affording 1.9 g of 4-[3-(4-tolyloxy)propyloxy]benzyl chloride.

Provenance & Evidence