HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67571854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9928639 | HCID 9928639 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 67571854 | HCID 67571854 | — |
Reaction Steps
0.55 g of 1-[4-(3-benzenesulfonylpropyloxy)benzyl]imidazole were dissolved in a mixed solvent of ether and DME, and hydrogen chloride gas was blown into the resultant solution for 5 minutes. The crystals precipitated were separated by filtration, thereby affording 0.49 g of 1-[4-(3-benzenesulfonylpropyloxy)benzyl]imidazole hydrochloride with a melting point of 194-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965743 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-b5d9078fef034f4fa6b6f6ec2e97886a |
| Source note | uspto-grants-1999_10 |