HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-ethyl-1,3,4-thiadiazole → HCID 21840882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-ethyl-1,3,4-thiadiazole | HCID 26444 | — |
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21840882 | HCID 21840882 | 64.9% |
Reaction Steps
A solution of 2-amino-5-ethyl-1,3,4-thiadiazole (42.6 g) and 4-iodobenzyl bromide (89.1 g) in ethanol (500 ml) was heated under reflux for 20 hours. After the reaction mixture was cooled, the crystals so precipitated were collected by filtration and then dried, whereby 83 g of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965738 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-65fdddd9ff5145c6ad0a3a98e8cad226 |
| Source note | uspto-grants-1999_10 |