HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-ethyl-1,3,4-thiadiazole → HCID 21840882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-ethyl-1,3,4-thiadiazole | HCID 26444 | — |
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21840882 | HCID 21840882 | 52.6% |
Reaction Steps
A solution of 2-amino-5-ethyl-1,3,4-thiadiazole (645 mg) and 4-iodobenzyl bromide (1.49 g) in methanol (5 ml) was heated under reflux for 2 hours. After the reaction mixture was cooled, the crystals so precipitated were collected by filtration and then dried, whereby 1.12 g of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965738 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-91f24d828ee1413ab32cc25f643fc4a6 |
| Source note | uspto-grants-1999_10 |