HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-ethyl-1,3,4-thiadiazole → HCID 21840882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-ethyl-1,3,4-thiadiazole | HCID 26444 | — |
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 21840882 | HCID 21840882 | 62.5% |
Reaction Steps
To isopropyl alcohol (10 ml) was added 2-amino-5-ethyl-1,3,4-thiadiazole (645 mg) and 4-iodobenzyl bromide (1.49 g), followed by heating under reflux for 2 hours. After the reaction mixture was cooled, the crystals so precipitated were collected by filtration and dried, whereby 1.33 g of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965738 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-97ff8b0d48124cc7b9a281ea7f6b10f5 |
| Source note | uspto-grants-1999_10 |