Hydroxyamine hydrochloride → HCID 21837527, compound

Participants

Reaction Steps

A mixture composed of 1 g (4.32 mmol) of the product obtained in Step 1, 1.26 g of hydroxylamine hydrochloride, 1.26 g of sodium acetate and 20 ml of ethanol are heated at reflux for 1 hour. After removal of the solvent by evaporation, the residue is taken up in 100 ml of methylene chloride, washed with water, dried and evaporated to yield 0.9 g of the expected product.

Provenance & Evidence