Hydrochloric Acid → HCID 21837525, compound

Participants

Reaction Steps

0.51 g (1.76 mmol) of the product obtained in Step 2 is treated at reflux for one night with 3 ml of 3N HCl. 1 ml of concentrated HCl is added and the whole is heated at reflux for 24 hours, allowed to cool, rendered basic with 2N NaOH and extracted 3 times with 30 ml of CH2Cl2 each time. The organic phases are washed and then dried. 0.32 g of the expected product is obtained. Yield: 73%.

Provenance & Evidence