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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1739809Generated: October 31, 2026

Diisopropylethylamine → HCID 9884687, compound

https://huagongshe.com/reaction/1739809

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
Reactant4-(4-Fluorobenzoyl)piperidineHCID 2724440—
ReactantHCID 13626982HCID 13626982—
SolventEthanolHCID 702—
ProductHCID 9884687HCID 9884687—

Reaction Steps

A solution of 3.5 g of 1-(3-methoxy-isoxazol-5-yl)-2-bromoethanol and 4.9 g of 4-(4'-fluorobenzoyl)piperidine and 5.4 ml of N-ethyldiisopropylamine in 160 ml of absolute ethanol was refluxed for 2 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05968955
Source datasetuspto-grants-1999_10
ORD IDord-1b97ea80d9d541fb83c5ad43ba27659e
Source noteuspto-grants-1999_10