HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloroacetic Acid → HCID 10620734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloroacetic Acid | HCID 6597 | — |
| Reactant | HCID 10521631 | HCID 10521631 | — |
| Product | HCID 10620734 | HCID 10620734 | 50% |
Reaction Steps
Analogously to the preparation of 62, 13.6 g (65%) 63 was obtained from 7.7 g (60 mmol) 4-chlorophenol and 18 g (60 mmol) 1,10-dibromodecane. 13.3 g (38.0 mmol) 63 was reacted with dichloroacetic acid according to example 9. 5.9 g (50%) 11, melting point 63-64° C. was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05968982 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-bd191b3bde6245b6814ab59bb6aff12a |
| Source note | uspto-grants-1999_10 |