HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloroacetic Acid → HCID 10549874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloroacetic Acid | HCID 6597 | — |
| Reactant | HCID 10761595 | HCID 10761595 | — |
| Product | HCID 10549874 | HCID 10549874 | 35% |
Reaction Steps
6.8 g (20 mmol) 92 was reacted with 10.3 g (80 mmol) dichloroacetic acid as in example 9. 2.8 g (35%) 41 with a melting point of 56-57° C. was obtained. The sodium salt obtained from 41 and pulverized NaOH in ethanol melted at 178° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05968982 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-cf2711c713c9437cb111e482b04e961f |
| Source note | uspto-grants-1999_10 |