HCID 21838184, compound → HCID 19363121, compound

Participants

Reaction Steps

Methyl 3-[(2-dimethylaminoethyl)carbamoyl]-5-trifluromethylsulfonyloxybenzoate trifluoromethanesulfonate (1.45 g) was dissolved in ethyl acetate (150 ml) and to the mixture water (50 ml) was added. The mixture was adjusted to pH 9 and two layers were separated. The organic layer was washed with brine, dried over magnesium sulfate and evaporated in vacuo to give methyl 3-[(2-dimethylaminoethyl)carbamoyl]-5-trifluoromethylsulfonyloxvbenzoate (1.14 g).

Provenance & Evidence