HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetaldehyde → HCID 69932725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetaldehyde | HCID 33 | — |
| Reactant | 6-tert-Butyl-m-cresol | HCID 6937 | — |
| Reactant | 2,6-Dimethylphenol | HCID 11335 | — |
| Product | HCID 69932725 | HCID 69932725 | 705.6% |
Reaction Steps
An amount of 195.5 g (0.16 mol) 2,6-xylenol (hereinafter referred to "26XY"), 65.7 g (0.4 mol) of 2-t-butyl-5-methylphenol and 174.4 g (1.0 mol) of an aqueous 45% chloroacetoaldehyde solution were charged in a flask and stilbene bisphenol (yellow crystal 208 g) was obtained according to the method described in R. H. Siebe, Liebigs, Ann. Chem., 730, 31 (1969).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969060 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-0725afe98c014446857d6cc129627bf5 |
| Source note | uspto-grants-1999_10 |