HRID1740389

反应详情

EQUATION

反应方程式

HRID 1740389 的结构方程式

PROCEDURE

实验过程

To an aqueous solution of 11.83 g of 1-(2-(2-propynyloxy)ethyl)piperazine dihydrochloride (water: 10 mL) was added aqueous sodium hydroxide solution, and the mixture was extracted with ethyl acetate. The organic layer was dried over anhydrous magnesium sulfate and evaporated to give 3.09 g of the title compound.

WORKUP

后处理

  1. extractionthe mixture was extracted with ethyl acetate
  2. dry with materialThe organic layer was dried over anhydrous magnesium sulfate
  3. customevaporated