HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 10970201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 131721411 | HCID 131721411 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10970201 | HCID 10970201 | 95.5% |
Reaction Steps
Into 2 mL of water was dissolved 180 mg of (S)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone (S)-(+)-mandelate, and the solution was desalted with sodium carbonate and extracted with ethyl acetate. The organic layer was dried over anhydrous magnesium sulfate and concentrated to give 120 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-d36e0e8c5fe644aaadd2d2382afec9d5 |
| Source note | uspto-grants-1999_10 |