HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 86754637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | MS-377 | HCID 9892249 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754637 | HCID 86754637 | 95% |
Reaction Steps
To a mixture of 379 mg of 47% hydrobromic acid aq. and 10 mL of ethanol was added a solution of 352 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of ethanol. The mixture was stirred at room temperature and then cooled. The precipitated solid was filtered and dried to give 488 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-91484dc786b5474bb8a80c3959bf4da8 |
| Source note | uspto-grants-1999_10 |