HuagongsheHuagongshe Chemistry Print Report · For research reference only
MS-377 free base → HCID 86754639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | MS-377 free base | HCID 9892249 | — |
| Reactant | Hydroxybenzenesulfonic acid | HCID 15619088 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754639 | HCID 86754639 | 154.3% |
Reaction Steps
To a solution of 176 mg of benzenesulfonic acid monohydrate in 10 mL of ethanol was added a solution of 352 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of ethanol. The mixture was concentrated. The residue was sludged with ethanol. The solid formed was filtered and dried to give 407 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-0ab2c4fd4869408dac0b5a45956d19f5 |
| Source note | uspto-grants-1999_10 |