HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Lactic Acid → HCID 131721412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Lactic Acid | HCID 107689 | — |
| Reactant | MS-377 | HCID 9892249 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131721412 | HCID 131721412 | 40.7% |
Reaction Steps
A mixture of 106 mg of 85% L-lactic acid aq. and 10 mL of ethyl acetate was added to a solution of 352 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of ethyl acetate. The mixture was stirred at room temperature and then concentrated. The residue was sludged with diethyl ether and dried to give 180 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-f72e2405dd194823a78308c99f505692 |
| Source note | uspto-grants-1999_10 |