HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Tartaric acid → HCID 86754644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | MS-377 free base | HCID 9892249 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754644 | HCID 86754644 | 59.6% |
Reaction Steps
To a solution of 300 mg of L-tartaric acid in 20 mL of ethanol was added a solution of 352 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of ethanol. The mixture was stirred at room temperature and cooled. The precipitated solid was filtered and dried to give 205 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-4ae401aace154bfda157373c40038613 |
| Source note | uspto-grants-1999_10 |