HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Tartaric acid → HCID 86754645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Tartaric acid | HCID 439655 | — |
| Reactant | MS-377 free base | HCID 9892249 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754645 | HCID 86754645 | 67.5% |
Reaction Steps
A solution of 75 mg of D-tartaric acid in 3 mL of ethanol was added to a solution of 176 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 3 mL of ethanol. The mixture was stirred at room temperature and cooled. The precipitated solid was filtered and dried to give 110 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-63fa68a4bfd545d5be9d9107933c31bd |
| Source note | uspto-grants-1999_10 |