HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → HCID 86754646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | MS-377 free base | HCID 9892249 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754646 | HCID 86754646 | 24.2% |
Reaction Steps
A solution of 591 mg of succinic acid in 20 mL of ethanol was added to a solution of 880 mg of (R)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 20 mL of ethanol. The mixture was stirred at room temperature and cooled. The precipitated solid was filtered and dried to give 356 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-3bb06041a79a45b7a7de032453fec4c5 |
| Source note | uspto-grants-1999_10 |