HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 70298834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5,5-dimethyl-2-cyclohexen-1-one | HCID 136680 | — |
| Reactant | HCID 22117818 | HCID 22117818 | — |
| Product | HCID 70298834 | HCID 70298834 | — |
Reaction Steps
Reaction of 3-amino-5,5-dimethyl-2-cyclohexen-1-one with 4-chloro-3-phenylsulphonylbenzaldehyde dimethyl acetal in an analogous manner to that described in Example 1 gave 9-[3-benzenesulphonyl-4-chlorophenyl]-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from dimethylformamide/water gave a yellow crystalline solid of melting point 252-254° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969139 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-0df284faaa3e485f8c44badbfedd9c3d |
| Source note | uspto-grants-1999_10 |