HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 54713534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | Methyl 4-hydroxy-2-oxo-1,2-dihydroquinoline-3-carboxylate | HCID 54676766 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54713534 | HCID 54713534 | — |
Reaction Steps
8.76 g (0.04 mol) of methyl 4-hydroxy-2-oxoquinoline-3-carboxylate was stirred with 3.7 g (0.05 mol) of tert-butylamine in 60 ml of ethanol in a miniautoclave for 8 hours at 150° C. under autogenous pressure. After cooling, the crystals were removed by suction filtration, washed with ligroin and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972841 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-fd9c455cfe9942979d5f98b368148a6a |
| Source note | uspto-grants-1999_10 |