Decylamine → HCID 21832979, compound

HRID 1740769Notes

Reaction equation

HRID 1740769 reaction equation
[CH2:1]([NH2:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[Cl:12][CH2:13][CH2:14][CH2:15][C:16]1[O:21][C:20](=[O:22])[C:19]2[CH:23]=[CH:24][CH:25]=[CH:26][C:18]=2[N:17]=1>>[Cl:12][CH2:13][CH2:14][CH2:15][C:16]([NH:17][C:18]1[CH:26]=[CH:25][CH:24]=[CH:23][C:19]=1[C:20]([NH:11][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:22])=[O:21]

Participants

3

Reactant 2

HCID 8916DecylamineHCID 21832987HCID 21832987, compound

Product 1

HCID 21832979HCID 21832979, compound

Conditions

Temperature
40 °C

Procedure

n-Decylamine (0.45 ml) was added to 2-(3-chloropropyl)-4H-3,I-benzoxazine-4-one (0.50 g). After being stirred for 45 minutes at 40° C., the reaction mixture was purified by silica gel column chromatography (silica gel 50 g, chloroform), thereby yielding 0.59 g of the aimed compound as light-yellow solid.

Workup

  1. customthe reaction mixture was purified by silica gel column chromatography (silica gel 50 g, chloroform)

Sources & evidence

ORD record
ord-3ef605c2997f485b9f2cec05f04dd0e7
Source dataset
uspto-grants-1999_10
Patent number
US05972929

Reaction notes

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