Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Decylamine | HCID 8916 | — |
| Reactant | HCID 21832987 | HCID 21832987 | — |
| Product | HCID 21832979 | HCID 21832979 | — |
Reaction Steps
n-Decylamine (0.45 ml) was added to 2-(3-chloropropyl)-4H-3,I-benzoxazine-4-one (0.50 g). After being stirred for 45 minutes at 40° C., the reaction mixture was purified by silica gel column chromatography (silica gel 50 g, chloroform), thereby yielding 0.59 g of the aimed compound as light-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05972929 |
|---|
| Source dataset | uspto-grants-1999_10 |
|---|
| ORD ID | ord-3ef605c2997f485b9f2cec05f04dd0e7 |
|---|
| Source note | uspto-grants-1999_10 |
|---|
