Nitrate → HCID 15435719, compound

Participants

Reaction Steps

To a solution of N-(14-mesyloxytetradecyl)-6-(4-methyl-1-piperazinyl)pyridine-3-carboxamide in toluene was added Amberlyst A-26 (a nitrate form) and the mixture was heated under reflux for 3 hours. The ion-exchange resin was filtered off and the filtrate was distilled off. The residue thus obtained was chromatographed over a silica gel column to afford 0.85 g of the title compound.

Provenance & Evidence