HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → 3-Nitrobenzaldoxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 3-Nitrobenzaldoxime | HCID 219132 | 79% |
Reaction Steps
3-Nitrobenzaldehyde (6 g, 40 mmol) was added to a solution of hydroxylamine (15 g, 216 mmol) in 5% aqueous sodium hydroxide solution (120 ml). Filtration and drying afforded the title compound as a white solid (5.23 g, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972937 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-7aa9eb363d12436c821bd3bfd0e50c0b |
| Source note | uspto-grants-1999_10 |