Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-6-methyl-2-phenylpyrimidine → HCID 21833464, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-6-methyl-2-phenylpyrimidine | HCID 598255 | — |
| 반응물 | 2-amino-N-methyl-N-phenylacetamide | HCID 11768899 | — |
| 반응물 | 2-amino-N,N-dipropyl-acetamide | HCID 12742481 | — |
| 반응물 | 4-Chloro-5,6-dimethyl-2-phenylpyrimidine | HCID 13487935 | — |
| 생성물 | HCID 21833464 | HCID 21833464 | — |
반응 단계
The same procedures as Example 1 are repeated except that 4-chloro-6-methyl-2-phenylpyrimidine and 2-amino-N-methyl-N-phenylacetamide are used instead of 4-chloro-5,6-dimethyl-2-phenylpyrimidine and 2-amino-N,N-dipropylacetamide, respectively. The product thus obtained is recrystallized from isopropanol to give the desired compound, m.p. 134-136° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05972946 |
| 출처 데이터셋 | uspto-grants-1999_10 |
| ORD ID | ord-4967eb9c61074c8bb7fc8bfb707b2e8c |
| 출처 메모 | uspto-grants-1999_10 |