HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21834421, compound → HCID 21834443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21834421 | HCID 21834421 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21834443 | HCID 21834443 | — |
Reaction Steps
A solution of 5-nitro-4-methyl-2-trimethylacetylaminopyridine (4.5 g, 18.97 mmol) in 50 mL of acetic acid containing 10% palladium/carbon was hydrogenated at atmospheric pressure for 48 h. The catalyst was removed by filtration and the filtrate was concentrated. The residue was coevaporated with toluene to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972975 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-e6fb60bf14fb4c2cb7d7927070233025 |
| Source note | uspto-grants-1999_10 |