HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21834430, compound → HCID 21834422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21834430 | HCID 21834430 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21834422 | HCID 21834422 | — |
Reaction Steps
A solution of 4-methyl-2-(trimethylacetyl)amino-5-(1-pentynyl)-pyridine (225 mg, 0.87 mmol) in ethyl acetate (4.5 mL) containing platinum oxide (45 mg) was hydrogenated at atmospheric pressure for 1.5 h. The catalyst was removed by filtration through a Millex-HV 0.45 um Filter Unit. Evaporation of the filtrate gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972975 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-fd33297981394917b02fba0ec53daf36 |
| Source note | uspto-grants-1999_10 |