HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 10219534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 21834412 | HCID 21834412 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 10219534 | HCID 10219534 | — |
Reaction Steps
By analogy to Example 56, Step B, 6-(2-aminoethyl)-4-methyl-2-(2,5-dimethylpyrrol-1-yl)pyridine was treated with 4.6 equivalents of hydroxylamine hydrochloride and 3.2 equivalents of potassium hydroxide in refluxing ethanol/water to yield 2-amino-6-(2-aminoethyl)-4-methylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972975 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-85e8a28d9f7247098a4885b97bf1aa96 |
| Source note | uspto-grants-1999_10 |