HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenesulfonyl chloride → Hmn 154
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Reactant | 2-[2-(4-Pyridyl)ethenyl]aniline | HCID 291341 | — |
| Product | Hmn 154 | HCID 6366736 | 21.1% |
Reaction Steps
Using 4.93 g of 2-[2-(4-pyridyl)ethenyl]aniline and 5.70 g of p-methoxybenzenesulfonyl chloride, the reaction and after-treatment procedure of Example 1 was otherwise carried out to give a crystal crop. This crystal crop was recrystallized from ethanol to provide 1.94 g of the title compound (light yellowish white prisms). m.p. 207-209° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972976 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-011027e162264871bba378f35458bd7d |
| Source note | uspto-grants-1999_10 |