HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (E)-4-[2-[2-[[(p-Methoxyphenyl)sulfonyl]amino]phenyl]ethenyl]pyridine Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hmn 154 | HCID 6366736 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (E)-4-[2-[2-[[(p-Methoxyphenyl)sulfonyl]amino]phenyl]ethenyl]pyridine Hydrochloride | HCID 21834473 | — |
Reaction Steps
One (1.00) compound obtained in Example 3A was dissolved in 100 ml of methanol followed by addition of hydrogen chloride gas-saturated ethereal solution of 5 times as much by volume under ice-cooling. The solvent was then evaporated off to provide 1.07 g of the title compound as yellow powders. m.p. 258-261° C. (decomp.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972976 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-f98c8cbec7424563b3f797c846a5c24e |
| Source note | uspto-grants-1999_10 |