Hydrochloric Acid → HCID 135584445, compound

HRID 1741019Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([NH:12][C:13]2[C:14](/[CH:19]=[CH:20]/[C:21]3[CH:26]=[CH:25][C:24]([OH:27])=[CH:23][CH:22]=3)=[N:15][CH:16]=[CH:17][CH:18]=2)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[ClH:28]>>[ClH:28].[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([NH:12][C:13]2[C:14](/[CH:19]=[CH:20]/[C:21]3[CH:22]=[CH:23][C:24]([OH:27])=[CH:25][CH:26]=3)=[N:15][CH:16]=[CH:17][CH:18]=2)(=[O:10])=[O:11])=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 135584444HCID 135584444, compound

Product 1

HCID 135584445HCID 135584445, compound

Procedure

A 0.74 g portion of the compound obtained in Example 39 was converted to the hydrochloride to provide 0.37 g of the title compound (yellow fine needles). m.p. 222-224° C. (decomp.)

Sources & evidence

ORD record: ord-9ccf3a19fc174edb93ff94d676a10a73
Source dataset: uspto-grants-1999_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05972976

Reaction notes

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