HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (E)-4-[2-[2-[N-(2-Methoxyethyl)-N-[(p-methoxyphenyl)sulfonyl]amino]phenyl]ethenyl]pyridine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | Hmn 154 | HCID 6366736 | — |
| Product | (E)-4-[2-[2-[N-(2-Methoxyethyl)-N-[(p-methoxyphenyl)sulfonyl]amino]phenyl]ethenyl]pyridine hydrochloride | HCID 21834528 | — |
Reaction Steps
Using 1.00 g of the compound obtained in Example 3A and 1-bromo-2-methoxyethane, the reaction and after-treatment procedure of Example 9 was otherwise carried out and the product was converted to the hydrochloride. By this procedure, 0.45 g of the title compound (amorphous) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972976 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-d0c4664749b346c7a3489d12d5768e85 |
| Source note | uspto-grants-1999_10 |