HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,6-Tetrahydro-1-methylpyridine-4-methanol → 1-Acetyl-8bromo-7-(1-methyl-1,2,3,6-tetrahydro-4-pyridyl)methoxy-2,3,4,5-tetrahydro-1H-benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,6-Tetrahydro-1-methylpyridine-4-methanol | HCID 118921 | — |
| Reactant | 1-Acetyl-8-bromo-7-hydroxy-2,3,4,5-tetrahydro-1H-benzazepine | HCID 21833802 | — |
| Product | 1-Acetyl-8bromo-7-(1-methyl-1,2,3,6-tetrahydro-4-pyridyl)methoxy-2,3,4,5-tetrahydro-1H-benzazepine | HCID 21833814 | — |
Reaction Steps
The title compound was prepared from 1-acetyl-8-bromo-7-hydroxy-2,3,4,5-tetrahydro-1H-benzazepine (D25) and 4-(hydroxymethyl)-1-methyl-1,2,3,6-tetrahydropyridine (D1) following the procedure of Description 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972951 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-b07d0eedd89a492c9b5f43be722ebfe3 |
| Source note | uspto-grants-1999_10 |