2-Bromo-1,2-diphenylethan-1-one → HCID 54089001, compound

HRID 1741402Notes

Reaction equation

HRID 1741402 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[CH2:6][N:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH:8]1[C:13]([OH:15])=[O:14].[C:19]1([C:25]([CH:27](Br)[C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[O:26])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[CH2:6][N:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH:8]1[C:13]([O:15][CH:27]([C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)[C:25](=[O:26])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:14]

Participants

3

Reactant 2

HCID 1026302-Bromo-1,2-diphenylethan-1-oneHCID 32970831-(3-Methoxy-benzyl)-piperidine-2-carboxylic acid

Product 1

HCID 54089001HCID 54089001, compound

Procedure

2-Oxo-1,2-diphenylethyl 1-(3-methoxybenzyl)-2-piperidinecarboxylate was prepared from 1-(3-methoxybenzyl)-2-piperidinecarboxylic acid and desyl bromide in a similar manner to that of Preparation 65. (+) APCI-MS (m/z): 444 (M+ +1) IR (Film): 1730, 1690, 1260 cm-1

Workup

  1. customof Preparation 65

Sources & evidence

ORD record
ord-35ce9a22fd504c0dac910ff98879dfb1
Source dataset
uspto-grants-1999_10
Patent number
US05972965

Reaction notes

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