Hydrochloric Acid → HCID 178499561, compound

HRID 1741463Notes

Reaction equation

HRID 1741463 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature (RT) for 18 hr. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customto stand at room temperature
  2. custom(RT)
  3. customfor 18 hr
  4. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-c62479efae384e0aabc4544384e9bb9e
Source dataset
uspto-grants-1999_10
Patent number
US05972984

Reaction notes

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