HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → HCID 18690859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 18690860 | HCID 18690860 | — |
| Product | HCID 18690859 | HCID 18690859 | — |
Reaction Steps
Methyl[3-amino-1,2-dihydro-2-oxo-6-phenyl-1-pyridyl]acetate (50f), was isolated (86%) as a grey solid: mp. 207-9° C.; IR (KBr) 3473, 3345, 1750, 1644, 1600, 1536, 1443, 1366, 1309, 1212, 1184, 1156; 1H NMR (d6 -DMSO) δ 7.30 (5H, m), 6.54 (1H, d), 6.03 (1H, d), 5.25 (2H, s), 4.49 (2H, s), 3.61 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05973111 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-ea93cc61e3bf490ea1239fb1113b645d |
| Source note | uspto-grants-1999_10 |