Pyridine → HCID 19010253, compound

Participants

Reaction Steps

Reactants (1) and (2) were added together in MeOH to ultimately result in about 20-26 wt-% of (3) in MeOH in a flask as illustrated above in Table I. All reactant mixtures A through D were divided by MeOH (abs), to reduce viscosity. The mixtures were allowed to stir overnight at room temperature. It was observed that Trials C and D had formed a white rubber polymer. Addition of methanol and stirring for 1 hour did not dissolve the polymeric material.

Provenance & Evidence