HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19007852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 9837778 | HCID 9837778 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 19007852 | HCID 19007852 | — |
Reaction Steps
A mixture of (2-fluorophenyl)(8-methyl-8-azabicyclo[3.2.1 ]octan-3-yl)methanone (29.5 g), hydroxylmine hydrochloride (16.5 g) and ammonium acetate (27.5 g) were heated in 80 ml of refluxing ethanol-water (3:1 mixture) for 19 hours. The mixture was and the precipitated product was collected (25.2g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05334599 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-7b2a7a50933c434d80cd14a15b94bcce |
| Source note | uspto-grants-1994_08 |