Hydrochloric Acid → HCID 20088026, compound

HRID 1741685Notes

Reaction equation

HRID 1741685 reaction equation
[CH3:1][C:2]([C:5]1[CH:10]=[C:9]([S:11][C@@H:12]2[CH2:16][CH2:15][CH2:14][C@H:13]2O)[CH:8]=[C:7]([C:18]([CH3:21])([CH3:20])[CH3:19])[C:6]=1[OH:22])([CH3:4])[CH3:3].[ClH:23]>>[Cl:23][CH:13]1[CH2:14][CH2:15][CH2:16][CH:12]1[S:11][C:9]1[CH:10]=[C:5]([C:2]([CH3:4])([CH3:3])[CH3:1])[C:6]([OH:22])=[C:7]([C:18]([CH3:21])([CH3:20])[CH3:19])[CH:8]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 15287672HCID 15287672, compound

Product 1

HCID 20088026HCID 20088026, compound

Procedure

The product of Example 7 (0.40 g, 0.0012 mole) was stirred with concentrated hydrochloric acid (5 ml) at room temperature for 20 hours. The solid was removed by filtration, washed with water and air dried to give the product as a white powder. The product was purified by silica gel chromatography to give a white solid. The structure was supported by NMR.

Workup

  1. customThe solid was removed by filtration
  2. washwashed with water and air
  3. customdried

Sources & evidence

ORD record
ord-be83eb6548484f64b87066365f5ec566
Source dataset
uspto-grants-1994_08
Patent number
US05334616

Reaction notes

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