HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 19010695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 2,4-Dichloro-6-methoxy-3,5-triazine | HCID 19267 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19010695 | HCID 19010695 | — |
Reaction Steps
The 2,4-dichloro-6-methoxy-s-triazine obtained according to Example A-3 is suspended, with partial solution, in 1000 parts by volume of acetone, 110 parts of thiophenol and 90 parts of sodium bicarbonate are added, and the reaction is carried out at about 20° C. After about 2 hours, the synthesis mixture is evaporated. The compound 2-chloro-4-methoxy-6-phenylthio-s-triazine is obtained as a powder containing electrolyte salt. It serves as a monochloro-triazine starting compound for the synthesis of dyestuffs according to the invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05334709 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-389dd7344ec74d699fc4f927eb6781e9 |
| Source note | uspto-grants-1994_08 |