1H-Pyrazol-3-amine, 5-methyl- → HCID 85412723, compound

Participants

Reaction Steps

Analogous to example 1, synthesis step 1, using 5.65 g (0.058 mol) of 3(5)-amino-5(3)-methyl-pyrazole and 10.6 g (0.058 mol) of 3-phenyl-propanehydroximoyl chloride. The oil obtained as raw product is dissolved in nitromethane in the cold and made to crystallise by scratching the side of the container. 8.2 g (57%) of 5-amino-3-methyl-1-(3-phenyl-propanehydroximoyl)-pyrazole with a m. pt. of 138°-140° C. are obtained.

Provenance & Evidence